diphenylacetylene-1-13C-d5

Base Information

Chemical Name:diphenylacetylene-1-13C-d5
CAS No.:828919-49-9
Molecular Formula:C₁₄H₁₀
Molecular Weight:189.143
Hs Code.:

Synonyms:diphenylacetylene-1-13C-d5

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Chemical Property of diphenylacetylene-1-13C-d5

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Technology Process of diphenylacetylene-1-13C-d5

There total 3 articles about diphenylacetylene-1-13C-d5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: C₁₃⁽¹³⁾CH₂⁽²⁾H₁₀O

: 828919-49-9
diphenylacetylene-1-13C-d5

Guidance literature:: C₁₃⁽¹³⁾CH₂⁽²⁾H₁₀O; With phosphorus pentachloride; In benzene; for 3h; Heating;

With sodium ethanolate; In ethanol; for 4h; Further stages.; Heating;
DOI:10.1021/ja070331c

Reference yield:

: C₁₄⁽¹³⁾CH₁₈⁽²⁾H₅NO

: 828919-49-9
diphenylacetylene-1-13C-d5

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: P^tBu₃; NaO^tBu / palladium acetate; Pd₂(dba)3 / tetrahydrofuran / 4 h / 60 °C

3.1: PCl₅ / benzene / 3 h / Heating

3.2: 33 percent / NaOEt / ethanol / 4 h / Heating

With tri-tert-butyl phosphine; phosphorus pentachloride; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; palladium diacetate; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/ja070331c

Reference yield:

: 942628-33-3
C₇⁽¹³⁾CH₃⁽²⁾H₅O

: 828919-49-9
diphenylacetylene-1-13C-d5

Guidance literature:: Multi-step reaction with 2 steps

1.1: P^tBu₃; NaO^tBu / palladium acetate; Pd₂(dba)3 / tetrahydrofuran / 4 h / 60 °C

2.1: PCl₅ / benzene / 3 h / Heating

2.2: 33 percent / NaOEt / ethanol / 4 h / Heating

With tri-tert-butyl phosphine; phosphorus pentachloride; sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; palladium diacetate; In tetrahydrofuran; benzene;
DOI:10.1021/ja070331c