3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

Base Information

Chemical Name:3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide
CAS No.:1358679-84-1
Molecular Formula:Br*C₂₀H₂₆NO₅
Molecular Weight:440.334
Hs Code.:

Synonyms:3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

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Chemical Property of 3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

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Technology Process of 3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

There total 1 articles about 3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 39931-77-6
pyridin-3-yl-acetic acid ethyl ester

: 65495-26-3
5-(2-bromo-ethyl)-1,2,3-trimethoxy-benzene

: 1358679-84-1
3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

Guidance literature:: at 80 ℃; for 3h; Inert atmosphere; Neat (no solvent);
DOI:10.1002/ejoc.201101058

Reference yield: 71.0%

: 1358679-84-1
3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

: 1358679-65-8
1-{[2-(3,4,5-trimethoxy-phenyl)-ethyl]-1,2,5,6-tetrahydro-pyridin-3-yl}-acetic acid ethyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/ejoc.201101058

Reference yield:

: 1358679-84-1
3-ethoxycarbonylmethyl-1-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-pyridinium bromide

: 1358679-69-2
1-{[2-(3,4,5-trimethoxy-phenyl)-ethyl]-1,4,5,6-tetrahydro-pyridin-3-yl}-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 20 h / 0 - 20 °C / Inert atmosphere

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 160 °C / Inert atmosphere; Microwave irradiation

With sodium tetrahydroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; acetonitrile;
DOI:10.1002/ejoc.201101058