N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Base Information

Chemical Name:N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester
CAS No.:78221-59-7
Molecular Formula:C₂₇H₂₈N₂O₆S
Molecular Weight:508.595
Hs Code.:

Synonyms:N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Suppliers and Price of N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

There total 3 articles about N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 78221-56-4
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine

: 88-75-5,78813-12-4
2-hydroxynitrobenzene

: 78221-59-7
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In pyridine; 1) 0 deg C, 30 min; 2) room temp., 12 h;
DOI:10.1135/cccc19810286

Reference yield:

: 78221-55-3
S-(2,4,6-trimethylbenzyl)-L-cysteine

: 78221-59-7
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / NaOH / H₂O / 0.5 h / Ambient temperature

2: 95 percent / dicydlohexylcarbodiimide / pyridine / 1) 0 deg C, 30 min; 2) room temp., 12 h

With sodium hydroxide; dicyclohexyl-carbodiimide; In pyridine; water;
DOI:10.1135/cccc19810286

Reference yield:

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 78221-59-7
N-benzyloxycarbonyl-S-(2,4,6-trimethylbenzyl)-L-cysteine o-nitrophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Na, liquid NH₃ / 1) 15 min; 2) 2 h

2: 69 percent / NaOH / H₂O / 0.5 h / Ambient temperature

3: 95 percent / dicydlohexylcarbodiimide / pyridine / 1) 0 deg C, 30 min; 2) room temp., 12 h

With sodium hydroxide; ammonia; sodium; dicyclohexyl-carbodiimide; In pyridine; water;
DOI:10.1135/cccc19810286