1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

Base Information

Chemical Name:1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene
CAS No.:186508-12-3
Molecular Formula:C₂₄H₃₀N₁₂S₃
Molecular Weight:582.781
Hs Code.:

Synonyms:1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

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Chemical Property of 1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

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Technology Process of 1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

There total 4 articles about 1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 17356-08-0
thiourea

: 186508-09-8
3-[3,5-Bis-(2,2-dicyano-ethyl)-2,4,6-trimethyl-phenyl]-2-cyano-propionitrile

: 186508-12-3
1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

Guidance literature:: With sodium ethanolate; In ethanol; Heating;
DOI:10.1135/cccc19961464

Reference yield:

: 21988-87-4
1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene

: 186508-12-3
1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / NaOEt, 2-nitropropane / ethanol; dimethylsulfoxide / Ambient temperature

2: 85 percent / piperidine / butan-1-ol

3: 97 percent / triethylammonium formate / dimethylformamide

4: 96 percent / NaOEt / ethanol / Heating

With piperidine; 2-nitropropane; sodium ethanolate; triethylammonium formate; In ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1135/cccc19961464

Reference yield:

: 119198-88-8
2,4,6-trimethylbenzene-1,3,5-tricarbaldehyde

: 186508-12-3
1,3,5-tris[4',6'-diamino-5'-methylenepyrimidine-2'-(1'H)-thione]-2,4,6-trimethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / piperidine / butan-1-ol

2: 97 percent / triethylammonium formate / dimethylformamide

3: 96 percent / NaOEt / ethanol / Heating

With piperidine; sodium ethanolate; triethylammonium formate; In ethanol; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1135/cccc19961464