O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

Base Information

Chemical Name:O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol
CAS No.:1611466-05-7
Molecular Formula:C₃₂H₃₄O₃
Molecular Weight:466.62
Hs Code.:

Synonyms:O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

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Chemical Property of O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

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Technology Process of O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

There total 5 articles about O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 3587-60-8
Benzyloxymethyl chloride

: 1611466-03-5
O,O-dibenzyl-4-i-butylresorcinol

: 1611466-05-7
O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

Guidance literature:: O,O-dibenzyl-4-i-butylresorcinol; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

Benzyloxymethyl chloride; In diethyl ether; hexane; for 2h; Inert atmosphere;
DOI:10.1002/chem.201304776

Reference yield: 40.0%

: 1611466-03-5
O,O-dibenzyl-4-i-butylresorcinol

: 1611466-05-7
O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether;
DOI:10.1021/acs.joc.6b00489

Reference yield:

: 29048-54-2
1-(2,4-dihydroxyphenyl)-2-methyl-1-propanone

: 1611466-05-7
O,O-dibenzyl-2-(benzyloxymethyl)-4-ibutylresorcinol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride; methyl orange; hydrogenchloride / methanol; water / 24 h

2.1: potassium carbonate / N,N-dimethyl-formamide

3.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / diethyl ether; hexane / 0.5 h / 0 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; methyl orange; sodium cyanoborohydride; potassium carbonate; In methanol; diethyl ether; hexane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201304776