Technology Process of C28H34N2O9S
There total 5 articles about C28H34N2O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: toluene-4-sulfonic acid / water; benzene / 1.5 h / 100 °C / Inert atmosphere
2: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere
3: silver(I) acetate / 4 h / 20 °C / Darkness; Inert atmosphere
4: methanol / 2 h / 0 - 20 °C / Inert atmosphere
5: sodium hydrogencarbonate / tetrahydrofuran / Inert atmosphere
With
silver(I) acetate; sodium hydrogencarbonate; Dess-Martin periodane; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; benzene;
DOI:10.1039/c4cc01692k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol / 2 h / 0 - 20 °C / Inert atmosphere
2: sodium hydrogencarbonate / tetrahydrofuran / Inert atmosphere
With
sodium hydrogencarbonate;
In
tetrahydrofuran; methanol;
DOI:10.1039/c4cc01692k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: silver(I) acetate / 4 h / 20 °C / Darkness; Inert atmosphere
2: methanol / 2 h / 0 - 20 °C / Inert atmosphere
3: sodium hydrogencarbonate / tetrahydrofuran / Inert atmosphere
With
silver(I) acetate; sodium hydrogencarbonate;
In
tetrahydrofuran; methanol;
DOI:10.1039/c4cc01692k