p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside
CAS No.:219488-93-4
Molecular Formula:C₂₈H₂₃Cl₄NO₈
Molecular Weight:643.305
Hs Code.:

Synonyms:p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

There total 7 articles about p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 219488-93-4
p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / TsOH / acetonitrile / 1 h

2: 1.) NaBH₃CN, 3 Angstroems MS, 2.) HCl / 1.) THF, rt, 3 h, 2.) THF, Et₂O, 0 deg C, 3 h

With hydrogenchloride; 3 Angstroems MS; sodium cyanoborohydride; toluene-4-sulfonic acid; In acetonitrile;
DOI:10.1021/jo981203x

Reference yield:

: 117-08-8
tetrachlorophthalic anhydride

: 219488-93-4
p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) pyridine, 22 deg C, 10 h, 2.) pyridine, 0 deg C, 1 h

2: 98 percent / BF₃*Et₂O / CH₂Cl₂ / 9 h / 20 °C

3: 86 percent / MeONa / methanol / 0.2 h / 22 °C

4: 77 percent / TsOH / acetonitrile / 1 h

5: 1.) NaBH₃CN, 3 Angstroems MS, 2.) HCl / 1.) THF, rt, 3 h, 2.) THF, Et₂O, 0 deg C, 3 h

With hydrogenchloride; 3 Angstroems MS; boron trifluoride diethyl etherate; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo981203x

Reference yield:

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 219488-93-4
p-methoxyphenyl 6-O-benzyl-2-deoxy-2-tetrachlorophthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) pyridine, 22 deg C, 10 h, 2.) pyridine, 0 deg C, 1 h

2: 98 percent / BF₃*Et₂O / CH₂Cl₂ / 9 h / 20 °C

3: 86 percent / MeONa / methanol / 0.2 h / 22 °C

4: 77 percent / TsOH / acetonitrile / 1 h

5: 1.) NaBH₃CN, 3 Angstroems MS, 2.) HCl / 1.) THF, rt, 3 h, 2.) THF, Et₂O, 0 deg C, 3 h

With hydrogenchloride; 3 Angstroems MS; boron trifluoride diethyl etherate; sodium methylate; sodium cyanoborohydride; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo981203x