(6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one

Base Information

Chemical Name:(6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one
CAS No.:1082553-12-5
Molecular Formula:C₂₀H₁₈N₂O₃
Molecular Weight:334.375
Hs Code.:

Synonyms:(6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one

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Chemical Property of (6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one

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Technology Process of (6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one

There total 2 articles about (6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 3-(6-(azetidin-1-ylcarbonyl)-4-hydroxy-1,2-dimethyl-1H-benzimidazol-5-yl)-1-(2-methylphenyl)propan-1-one

: (1R)-3-[6-(azetidin-1-ylcarbonyl)-4-hydroxy-1,2-dimethyl-1H-benzimidazol-5-yl]-1-(2-methylphenyl)propan-1-ol

: 1082553-12-5
(6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one

: 6-(azetidin-1-ylcarbonyl)-5-[(3S)-3-hydroxy-3-(2-methylphenyl)propyl]-1,2-dimethyl-1H-benzimidazol-4-ol

Guidance literature:: With potassium hydroxide; hydrogen; RuCl₂[(S)-Xyl-P-Phos][(S)-DAIPEN]; In isopropyl alcohol; tert-butyl alcohol; under 18751.9 Torr; Title compound not separated from byproducts.; Heating;
DOI:10.1016/j.tetasy.2008.08.022

Reference yield: 17.0%

: 917957-35-8
4-hydroxy-N,N,1,2-tetramethyl-5-[3-(2-methylphenyl)-3-oxopropyl]-1H-benzimidazole-6-carboxamide

: 1082553-12-5
(6Z)-8-hydroxy-6-[hydroxy(2-methylphenyl)methylene]-2,3-dimethyl-6,7-dihydroindeno[5,6-d]imidazol-5(3H)-one

: 4-hydroxy-5-[3-hydroxy-3-(2-methylphenyl)propyl]-N,N,1,2-tetramethyl-1H-benzimidazole-6-carboxamide

Guidance literature:: With potassium tert-butylate; hydrogen; RuCl₂[(S)-Xyl-P-Phos][(S)-DAIPEN]; In isopropyl alcohol; tert-butyl alcohol; at 70 ℃; for 22h; under 60006 Torr;
DOI:10.1016/j.tetasy.2008.08.022