5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

Base Information

Chemical Name:5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal
CAS No.:123002-59-5
Molecular Formula:C₁₇H₂₈O₂Si
Molecular Weight:292.494
Hs Code.:

Synonyms:5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

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Chemical Property of 5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

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Technology Process of 5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

There total 1 articles about 5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: [4-(4-Benzenesulfonylmethyl-[1,3]dioxolan-2-yl)-1-phenyl-butoxy]-tert-butyl-dimethyl-silane

: 123002-59-5
5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 36h; Ambient temperature;
DOI:10.1016/S0040-4039(98)00209-3

Reference yield:

: 123002-59-5
5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

: 123002-78-8,123002-79-9
<2R(S),3S(R)>-2-<(phenylthio)carbonyl>-6-phenyltetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) potassium tert-butoxide / 1.) tert-butyl alcohol, THF, 0 deg C, 15 min, 2.) tert-butyl alcohol, THF, RT

2: methanesulfonyl chloride, ethyldiisopropylamine / CH₂Cl₂ / 1.) -78 deg C, 10 min, 2.) -30 deg C, 10 min

With potassium tert-butylate; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00280a058

Reference yield:

: 123002-59-5
5-(tert-Butyl-dimethyl-silanyloxy)-5-phenyl-pentanal

: 123002-68-6
1-<(tert-butyldimethylsilyl)oxy>-1-phenyl-6-nitro-6-(phenylthio)-(Z)-5-hexene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium tert-butoxide / 1.) tert-butyl alcohol, THF, 0 deg C, 15 min, 2.) tert-butyl alcohol, THF, RT

2: methanesulfonyl chloride, ethyldiisopropylamine / CH₂Cl₂ / 1.) -78 deg C, 10 min, 2.) -30 deg C, 10 min

With potassium tert-butylate; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00280a058