N-picolinoyl-N'-thiobenzoyl hydrazine

Base Information

Chemical Name:N-picolinoyl-N'-thiobenzoyl hydrazine
CAS No.:448963-68-6
Molecular Formula:C₁₃H₁₁N₃OS
Molecular Weight:257.316
Hs Code.:

Synonyms:N-picolinoyl-N'-thiobenzoyl hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-picolinoyl-N'-thiobenzoyl hydrazine

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Technology Process of N-picolinoyl-N'-thiobenzoyl hydrazine

There total 1 articles about N-picolinoyl-N'-thiobenzoyl hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1452-63-7
picolinic acid hydrazide

: 942-91-6
Carboxymethyl dithiobenzoate

: 448963-68-6
N-picolinoyl-N'-thiobenzoyl hydrazine

Guidance literature:: picolinic acid hydrazide; Carboxymethyl dithiobenzoate; With sodium hydroxide; In methanol; at 20 ℃;

With acetic acid; In methanol;
DOI:10.1016/j.molstruc.2014.01.043

Reference yield: 78.0%

: 448963-68-6
N-picolinoyl-N'-thiobenzoyl hydrazine

: 15311-23-6
2-phenyl-5-(pyridin-2-yl)-1,3,4-thiadiazole

Guidance literature:: With manganese (II) nitrate tetrahydrate; In ethanol; water; for 1h;
DOI:10.1016/j.molstruc.2013.09.051

Reference yield: 60.0%

: nickel(II) dichloride hydrate

: 448963-68-6
N-picolinoyl-N'-thiobenzoyl hydrazine

: Ni⁽²⁺⁾*SC(C₆H₅)NNHC(O)C₅H₄N^(1-)*Cl^(1-) = Ni(SC(C₆H₅)NNHC(O)C₅H₄N)Cl

Guidance literature:: With HCl; In ethanol; byproducts: H2O, HCl; mixing soln. NiCl2*xH2O in EtOH and N-picolinoyl-N'-thiobenzoyl hydrazine (1:1 mol) with 0.5 M HCl at 25°C; filtered off; washed; dried (vac.); elem. anal.;
DOI:10.1081/SIM-120004441