Technology Process of C28H33N7O7
There total 9 articles about C28H33N7O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 0 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C
1.2: 20 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
3.1: sodium hydroxide; water / methanol / 20 °C
4.1: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 - 50 °C
5.1: triethylamine / dichloromethane / 0 - 20 °C
With
sodium hydroxide; thionyl chloride; water; hydrogen; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
palladium 10% on activated carbon;
In
methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h
2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C
2.2: 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C
4.1: sodium hydroxide; water / methanol / 20 °C
5.1: thionyl chloride / N,N-dimethyl-formamide / 0.5 h / 0 - 50 °C
6.1: triethylamine / dichloromethane / 0 - 20 °C
With
sodium hydroxide; thionyl chloride; tetrabutyl ammonium fluoride; water; hydrogen; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;