(+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate

Base Information

• Chemical Name: (+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate
• CAS No.: 1228675-28-2
• Molecular Formula: C₁₈H₂₄N₂O₄
• Molecular Weight: 332.4

Synonyms:(+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate

Chemical Property of (+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

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Technology Process of (+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate

There total 1 articles about (+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

diiodomethane (75-11-6) + 1-benzyl 4-tert-butyl 2,3-dihydropyrazine-1,4-dicarboxylate (1228675-27-1) → (+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate (1228675-28-2)

Guidance literature:

diiodomethane; 1-benzyl 4-tert-butyl 2,3-dihydropyrazine-1,4-dicarboxylate; With diethylzinc; In diethyl ether; hexane; at 20 ℃; for 18h; Inert atmosphere;

With ammonium chloride; In diethyl ether; hexane; water; Saturated solution;

DOI:10.1016/j.tet.2010.02.046

Reference yield: 94.0%

(+/-)-2-benzyl 5-tert-butyl 2,5-diazabicyclo[4.1.0]heptane-2,5-dicarboxylate (1228675-28-2) → (+/-)-5-(benzyloxycarbonyl)-2,5-diazabicyclo[4.1.0]heptane hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; diethyl ether; at 20 ℃; for 18h;

DOI:10.1016/j.tet.2010.02.046

upstream raw materials:

diiodomethane

1-benzyl 4-tert-butyl 2,3-dihydropyrazine-1,4-dicarboxylate

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