Technology Process of C23H28O4
There total 4 articles about C23H28O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
DOI:10.1055/s-2007-982556
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / pyridinium chlorochromate; NaOAc / 3 h / 20 °C
2: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 20 °C
With
sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridinium chlorochromate;
In
tetrahydrofuran;
DOI:10.1055/s-2007-982556
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; water / 15 h / 55 °C
2: 100 percent / pyridinium chlorochromate; NaOAc / 3 h / 20 °C
3: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 20 °C
With
water; sodium acetate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridinium chlorochromate;
In
tetrahydrofuran;
DOI:10.1055/s-2007-982556