Technology Process of C23H30O5S
There total 8 articles about C23H30O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-toluenesulfonic acid / acetone; H2O / 20 h / Heating
2: 73 percent / methanol, NaH / diethyl ether / 20 h / Ambient temperature
3: 53 percent / methylsulfonyl azide, triethylamine / acetonitrile / 5 h / Ambient temperature
4: 37 percent / benzene / 3 h / Irradiation
5: pyridine
With
pyridine; methanol; sodium hydride; toluene-4-sulfonic acid; triethylamine; Methanesulfonyl azide;
In
diethyl ether; water; acetone; acetonitrile; benzene;
DOI:10.1021/ja00228a029
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / methanol, NaH / diethyl ether / 20 h / Ambient temperature
2: 53 percent / methylsulfonyl azide, triethylamine / acetonitrile / 5 h / Ambient temperature
3: 37 percent / benzene / 3 h / Irradiation
4: pyridine
With
pyridine; methanol; sodium hydride; triethylamine; Methanesulfonyl azide;
In
diethyl ether; acetonitrile; benzene;
DOI:10.1021/ja00228a029
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 53 percent / methylsulfonyl azide, triethylamine / acetonitrile / 5 h / Ambient temperature
2: 37 percent / benzene / 3 h / Irradiation
3: pyridine
With
pyridine; triethylamine; Methanesulfonyl azide;
In
acetonitrile; benzene;
DOI:10.1021/ja00228a029
