N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

Base Information

Chemical Name:N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide
CAS No.:1297273-57-4
Molecular Formula:C₃₇H₅₀N₄O₄S
Molecular Weight:646.894
Hs Code.:

Synonyms:N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

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Chemical Property of N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

Chemical Property:

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Technology Process of N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

There total 4 articles about N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 35386-24-4
1-(2-Methoxyphenyl)piperazine

: 1297273-56-3
C₂₇H₃₈N₂O₆S₂

: 1297273-57-4
N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

Guidance literature:: With potassium carbonate; sodium iodide; In acetonitrile; Reflux;
DOI:10.1016/j.bmc.2011.01.053

Reference yield:

: 79640-92-9,64781-19-7
(+/-)-11-Hydroxy-N-propylnoraporphine

: 1297273-57-4
N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammomium bromide; sodium hydroxide / water / 1 h / 20 °C

2: butan-1-ol / 24 h / Reflux

3: triethylamine / dichloromethane / 2.25 h / 0 - 20 °C

4: potassium carbonate; sodium iodide / acetonitrile / Reflux

With tetrabutylammomium bromide; potassium carbonate; triethylamine; sodium iodide; sodium hydroxide; In dichloromethane; water; acetonitrile; butan-1-ol;
DOI:10.1016/j.bmc.2011.01.053

Reference yield:

: 1297273-53-0
C₂₂H₂₆ClNO

: 1297273-57-4
N-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-N-(3-(N-propylnoraporphin-11-yloxy)-propyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: butan-1-ol / 24 h / Reflux

2: triethylamine / dichloromethane / 2.25 h / 0 - 20 °C

3: potassium carbonate; sodium iodide / acetonitrile / Reflux

With potassium carbonate; triethylamine; sodium iodide; In dichloromethane; acetonitrile; butan-1-ol;
DOI:10.1016/j.bmc.2011.01.053