Technology Process of C24H40SiO3
There total 6 articles about C24H40SiO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
at -110 ℃;
DOI:10.1055/s-2007-986647
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 100 percent / CH2Cl2 / 20 °C
2: 95 percent / imidazole / CH2Cl2 / 20 °C
3: 98 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
4: 94 percent / Dess-Martin periodinane / CH2Cl2 / 20 °C
5: 68 percent / sodium hexamethyldisilazide / tetrahydrofuran / -110 °C
With
1H-imidazole; lithium aluminium tetrahydride; sodium hexamethyldisilazane; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane;
5: Wittig reaction;
DOI:10.1055/s-2007-986647
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / imidazole / CH2Cl2 / 20 °C
2: 98 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
3: 94 percent / Dess-Martin periodinane / CH2Cl2 / 20 °C
4: 68 percent / sodium hexamethyldisilazide / tetrahydrofuran / -110 °C
With
1H-imidazole; lithium aluminium tetrahydride; sodium hexamethyldisilazane; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane;
4: Wittig reaction;
DOI:10.1055/s-2007-986647