5-methyl-6,8-diphenylindolizine

Base Information

Chemical Name:5-methyl-6,8-diphenylindolizine
CAS No.:1443442-31-6
Molecular Formula:C₂₁H₁₇N
Molecular Weight:283.373
Hs Code.:

Synonyms:5-methyl-6,8-diphenylindolizine

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Chemical Property of 5-methyl-6,8-diphenylindolizine

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Technology Process of 5-methyl-6,8-diphenylindolizine

There total 5 articles about 5-methyl-6,8-diphenylindolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1,3-diphenyl-4-(1H-pyrrol-1-yl)pent-1-yn-3-ol

: 1443442-31-6
5-methyl-6,8-diphenylindolizine

Guidance literature:: With silver(I) hexafluorophosphate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I); In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1039/c7ob02102j

Reference yield: 85.0%

: 64608-69-1
2-(1H-pyrrol-1-yl)propanenitrile

: 94-41-7
benzalacetophenone

: 1443442-31-6
5-methyl-6,8-diphenylindolizine

Guidance literature:: 2-(1H-pyrrol-1-yl)propanenitrile; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

benzalacetophenone; In tetrahydrofuran; Further stages; Inert atmosphere;
DOI:10.1021/jo400992n

Reference yield:

: 90490-62-3
1-phenyl-2-(1H-pyrrol-1-yl)ethan-1-one

: 1443442-31-6
5-methyl-6,8-diphenylindolizine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / 0 °C / Inert atmosphere; Schlenk technique

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere; Schlenk technique

2.2: 1 h / 20 °C / Inert atmosphere; Schlenk technique

3.1: silver(I) hexafluorophosphate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I) / dichloromethane / 1 h / 20 °C / Inert atmosphere; Schlenk technique; Glovebox

With n-butyllithium; silver(I) hexafluorophosphate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I); sodium hydride; In tetrahydrofuran; hexane; dichloromethane; mineral oil;
DOI:10.1039/c7ob02102j