(2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

Base Information

Chemical Name:(2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol
CAS No.:132938-61-5
Molecular Formula:C₂₈H₄₀N₂O₇
Molecular Weight:516.635
Hs Code.:

Synonyms:(2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

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Chemical Property of (2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

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Technology Process of (2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

There total 3 articles about (2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 132938-52-4
(2R,4S,5R,6R)-6-Benzyloxy-5-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-4-hydroxy-2-methyl-dihydro-pyran-3-one O-benzyl-oxime

: 132938-53-5
(2R,3R,4S,5S,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

: 132938-61-5
(2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

Guidance literature:: With titanium(IV) isopropylate; diphenylsilane; In dichloromethane; at 25 ℃; for 1h;

Reference yield:

: 132938-51-3
((3S,4S,6S)-6-{(2R,3R,4S,6R)-2-Benzyloxy-5-[(Z)-benzyloxyimino]-4-hydroxy-6-methyl-tetrahydro-pyran-3-yloxy}-4-methoxy-tetrahydro-pyran-3-yl)-ethyl-carbamic acid 9H-fluoren-9-ylmethyl ester

: 132938-61-5
(2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₂NH / tetrahydrofuran / 2 h / 25 °C

2: 92 percent / Ti(OiPr)4, Ph₂SiH₂ / CH₂Cl₂ / 1 h / 25 °C

With titanium(IV) isopropylate; diphenylsilane; diethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 132938-50-2
((3S,4S,6S)-6-{(2R,3R,4S,6R)-2-Benzyloxy-5-[(E)-benzyloxyimino]-6-methyl-4-triethylsilanyloxy-tetrahydro-pyran-3-yloxy}-4-methoxy-tetrahydro-pyran-3-yl)-ethyl-carbamic acid 9H-fluoren-9-ylmethyl ester

: 132938-61-5
(2R,3R,4S,5R,6R)-2-Benzyloxy-5-benzyloxyamino-3-((2S,4S,5S)-5-ethylamino-4-methoxy-tetrahydro-pyran-2-yloxy)-6-methyl-tetrahydro-pyran-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / HF*pyridine / CH₂Cl₂; tetrahydrofuran / 0.33 h / 0 °C

2: 98 percent / Et₂NH / tetrahydrofuran / 2 h / 25 °C

3: 92 percent / Ti(OiPr)4, Ph₂SiH₂ / CH₂Cl₂ / 1 h / 25 °C

With titanium(IV) isopropylate; diphenylsilane; pyridine hydrogenfluoride; diethylamine; In tetrahydrofuran; dichloromethane;