[OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄

Base Information

Chemical Name:[OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄
CAS No.:83114-82-3
Molecular Formula:C₃₉H₃₀ClO₃OsP₂*ClO₄
Molecular Weight:933.717
Hs Code.:

[OsCl(CO)3(P(C<sub>6</sub>H<sub>5</sub>)3)2]<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[OsCl(CO)3(P(C<sub>6</sub>H<sub>5</sub>)3)2]ClO<sub>4</sub>

Synonyms:[OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄

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Chemical Property of [OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄

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Technology Process of [OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄

There total 1 articles about [OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.1%

: 83076-18-0
[OsCl(CO)2(P(C₆H₅)3)3]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)2(P(C₆H₅)3)3]ClO₄

: 83114-82-3
[OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄

Guidance literature:: With CO; In dichloromethane; under CO at 80°C for 2 h; hexane added at room temp., CH2Cl2 removed;
DOI:10.1016/S0022-328X(00)81212-7

Reference yield:

: 83114-82-3
[OsCl(CO)3(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[OsCl(CO)3(P(C₆H₅)3)2]ClO₄

: 54933-53-8,25702-67-4
Os(P(C₆H₅)3)2(CO)2HCl

: 68170-74-1,62793-26-4
Os(CHO)Cl(CO)2(P(C₆H₅)3)2

Guidance literature:: With NaBH₄; In ethanol; dichloromethane; filtered soln. of excess of NaBH4 in EtOH added to complex soln. in CH2Cl2, stirred for 5 min; CH2Cl2 removed (vac., no heat), crystals collected, washed with H2O andEtOH, detected by IR;
DOI:10.1016/S0022-328X(00)81212-7