Bicyclo[2.2.1]hept-2-ene, 7-(dichloromethoxy)-, (7-anti)- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]hept-2-ene, 7-(dichloromethoxy)-, (7-anti)- (9CI)
• CAS No.: 738586-77-1
• Molecular Formula: C₈H₁₀Cl₂O
• Molecular Weight: 193.073
• Mol file: 738586-77-1.mol

Synonyms:Bicyclo[2.2.1]hept-2-ene, 7-(dichloromethoxy)-, (7-anti)- (9CI)

Chemical Property of Bicyclo[2.2.1]hept-2-ene, 7-(dichloromethoxy)-, (7-anti)- (9CI)

Chemical Property:

• Boiling Point: 240.2±40.0 °C(Predicted)
• Density: 1.29±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bicyclo[2.2.1]hept-2-ene, 7-(dichloromethoxy)-, (7-anti)- (9CI)

There total 2 articles about Bicyclo[2.2.1]hept-2-ene, 7-(dichloromethoxy)-, (7-anti)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-((1S,4R,7S)-Bicyclo[2.2.1]hept-2-en-7-yloxy)-3-chloro-3H-diazirine → anti-7-norbornenyl chloride (1121-10-4) + Formic acid (1S,4R,7S)-bicyclo[2.2.1]hept-2-en-7-yl ester + (1S,4R,7S)-7-Dichloromethoxy-bicyclo[2.2.1]hept-2-ene (738586-77-1,740804-81-3)

Guidance literature:

With water; In chloroform-d1; at 25 ℃; UV-irradiation;

DOI:10.1016/j.tetlet.2004.04.134

Reference yield:

ant-7-norbornenol (694-70-2) → (1S,4R,7S)-7-Dichloromethoxy-bicyclo[2.2.1]hept-2-ene (738586-77-1,740804-81-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: MeSO₃H

1.2: NaOCl

2.1: 4 percent Chromat_. / water / CDCl₃ / 25 °C / UV-irradiation

With methanesulfonic acid; water; In chloroform-d1;

DOI:10.1016/j.tetlet.2004.04.134

upstream raw materials:

ant-7-norbornenol

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