3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine

Base Information

Chemical Name:3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine
CAS No.:1374986-94-3
Molecular Formula:C₂₂H₂₀Cl₂N₂
Molecular Weight:383.32
Hs Code.:

Synonyms:3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine

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Technology Process of 3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine

There total 2 articles about 3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1374986-89-6
N,N'-bis(4-chloro-2,6-dimethylphenyl)benzene-1,2-diamine

: 1374986-94-3
3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine

Guidance literature:: With sodium periodate; silica gel; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/adsc.201100890

Reference yield:

: 24596-18-7
4-chloro-2,6-dimethylaniline

: 583-53-9
2,3-dibromobenzene

: 1374986-94-3
3-chloro-5-(4-chloro-2,6-dimethylphenyl)-1,4a-dimethyl-4a,5-dihydrophenazine

Guidance literature:: Multi-step reaction with 2 steps

1: tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate / toluene / 110 °C / Inert atmosphere

2: sodium periodate; silica gel / dichloromethane / 24 h / 20 °C

With sodium periodate; tri-tert-butyl phosphine; palladium diacetate; silica gel; sodium t-butanolate; In dichloromethane; toluene; 1: Buchwald-Hartwig amination;
DOI:10.1002/adsc.201100890