(α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Base Information

Chemical Name:(α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle
CAS No.:122082-72-8
Molecular Formula:C₁₉H₂₉NO₃
Molecular Weight:319.444
Hs Code.:

Synonyms:(α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

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Chemical Property of (α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

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Technology Process of (α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

There total 6 articles about (α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 122082-71-7
<α-(N-benzyloxycarbonyl N-methyl amino) methoxy-4 benzyl>-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

: 122082-72-8
(α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 57078-08-7,57129-25-6,61490-75-3,93781-25-0,116696-95-8,116696-96-9,145415-55-0,145415-56-1,82801-37-4
acide cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

: 122082-72-8
(α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: Multi-step reaction with 6 steps

1: diethyl ether

2: 77 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

3: 47 percent / Al/Hg, 5percent HgCl / ethanol; H₂O / 2 h

4: 97 percent / Na / H₂O / 40 h / 0 - 20 °C

5: 77 percent / NaH / dimethylformamide / 3 h

6: 86 percent / H₂ / 10percent Pd/C / methanol

With pyridine; aluminum amalgam; hydroxylamine hydrochloride; hydrogen; sodium; sodium hydride; mercury(II) chloride; palladium on activated charcoal; In methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 93740-32-0,93740-33-1,122082-22-8
ester methylique de l'acide cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

: 122082-72-8
(α-methylamino methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylate de methyle

Guidance literature:: Multi-step reaction with 5 steps

1: 77 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

2: 47 percent / Al/Hg, 5percent HgCl / ethanol; H₂O / 2 h

3: 97 percent / Na / H₂O / 40 h / 0 - 20 °C

4: 77 percent / NaH / dimethylformamide / 3 h

5: 86 percent / H₂ / 10percent Pd/C / methanol

With pyridine; aluminum amalgam; hydroxylamine hydrochloride; hydrogen; sodium; sodium hydride; mercury(II) chloride; palladium on activated charcoal; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(88)90091-8