1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Base Information

Chemical Name:1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene
CAS No.:88628-77-7
Molecular Formula:C₃₂H₃₅NO₆
Molecular Weight:529.633
Hs Code.:

Synonyms:1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Suppliers and Price of 1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Chemical Property:

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Technology Process of 1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

There total 12 articles about 1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 93622-56-1
1-<3-(o-ethoxycarbonylphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

: 88628-77-7
1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Guidance literature:: With potassium hydroxide; In ethanol; Heating; overnight;
DOI:10.1246/bcsj.57.1976

Reference yield:

: 98-29-3
4-tert-Butylcatechol

: 88628-77-7
1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) powdered potassium carbonate; 2.) KI / 1.) 70 deg C, 24 h, DMF; 2.) 70 deg C, 24 h

2: 76 percent / thionyl chloride / benzene; pyridine / 10 h / Heating

3: 1.) t-BuOK / 1.) DMF; 2.) 70 deg C, 42 h

4: 62 percent / NaH / dimethylformamide / 48 h / 70 °C

5: 79 percent / KOH / ethanol / Heating; overnight

With potassium hydroxide; thionyl chloride; potassium tert-butylate; sodium hydride; potassium carbonate; potassium iodide; In pyridine; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1246/bcsj.57.1976

Reference yield:

: 83557-01-1
1,2-bis(3-hydroxypropoxy)-4-t-butylbenzene

: 88628-77-7
1-<3-(o-carboxyphenoxy)propoxy>-2-<3-(8-quinolyloxy)propoxy>-4-t-butylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / thionyl chloride / benzene; pyridine / 10 h / Heating

2: 1.) t-BuOK / 1.) DMF; 2.) 70 deg C, 42 h

3: 62 percent / NaH / dimethylformamide / 48 h / 70 °C

4: 79 percent / KOH / ethanol / Heating; overnight

With potassium hydroxide; thionyl chloride; potassium tert-butylate; sodium hydride; In pyridine; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1246/bcsj.57.1976