Technology Process of C17H18N4O2
There total 7 articles about C17H18N4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 2 h / 20 °C
2.1: iron; acetic acid / 50 - 80 °C
3.1: orthoformic acid triethyl ester / 4 h / 100 °C
4.1: caesium carbonate / tert-butyl alcohol / 0.33 h / Inert atmosphere
4.2: 5 h / Reflux
With
iron; caesium carbonate; acetic acid; orthoformic acid triethyl ester;
In
tetrahydrofuran; tert-butyl alcohol;
- Guidance literature:
-
3-amino-4-ethylbenzoic acid methyl ester; 6-chloro-1-methyl-1H-imidazo[4,5-c]pyridine;
With
caesium carbonate;
In
tert-butyl alcohol;
for 0.333333h;
Inert atmosphere;
With
chloro[2-(dicyclohexylphosphino)-3 ,6-dimethoxy-2’,4’, 6’-triisopropyl- 1,1’-biphenyl] [2-(2-aminoethyl)phenyl]palladium(II); ruphos;
In
tert-butyl alcohol;
for 5h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: iron; acetic acid / 50 - 80 °C
2.1: orthoformic acid triethyl ester / 4 h / 100 °C
3.1: caesium carbonate / tert-butyl alcohol / 0.33 h / Inert atmosphere
3.2: 5 h / Reflux
With
iron; caesium carbonate; acetic acid; orthoformic acid triethyl ester;
In
tert-butyl alcohol;