C₃₅H₄₈O₁₃

Base Information Edit

Chemical Name:C₃₅H₄₈O₁₃
CAS No.:1018988-65-2
Molecular Formula:C₃₅H₄₈O₁₃
Molecular Weight:676.758
Hs Code.:
Mol file:1018988-65-2.mol

C<sub>35</sub>H<sub>48</sub>O<sub>13</sub>

Synonyms:C₃₅H₄₈O₁₃

Suppliers and Price of C₃₅H₄₈O₁₃

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₅H₄₈O₁₃ Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₅H₄₈O₁₃

There total 20 articles about C₃₅H₄₈O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1018988-55-0
C₁₇H₂₀(OH)2(OCOCH₃)2(CH₂OCOCH₃)(CH₃)(OCOC₆H₄OCH₃)(CHCH₂)

: 1018988-65-2
C₃₅H₄₈O₁₃

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃; for 5h;
DOI:10.1002/anie.200704959

Reference yield: 76.0%

: 1018988-53-8
C₃₅H₄₆O₁₃

: 1018988-65-2
C₃₅H₄₈O₁₃

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1002/anie.200704959

Reference yield:

: 1018988-59-4
C₅₂H₆₆O₇Si₂

: 1018988-65-2
C₃₅H₄₈O₁₃

Guidance literature:: Multi-step reaction with 18 steps

1.1: sodium tetrahydroborate / ethanol / 2 h / -78 °C / Inert atmosphere

2.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 39 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

5.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

6.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 13 °C / Inert atmosphere

7.1: lithium borohydride / tetrahydrofuran / Inert atmosphere; Reflux

7.2: 4 h / 20 °C / Inert atmosphere

8.1: lithium borohydride / tetrahydrofuran / 26.5 h / 20 °C / Inert atmosphere; Reflux

8.2: 4 h / 20 °C / Inert atmosphere

9.1: water; acetic acid / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

10.1: dmap / pyridine; dichloromethane / 24 h / 20 °C / Inert atmosphere

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

12.1: peracetic acid; mercury(II) diacetate; acetic acid / 4 h / 20 °C / Inert atmosphere

13.1: 1H-imidazole / dichloromethane / 4 h / 0 °C / Inert atmosphere

14.1: dmap / pyridine; dichloromethane / 0 - 40 °C / Inert atmosphere

15.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

16.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

17.1: Wilkinson's catalyst; triphenylphosphine; isopropyl alcohol / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

18.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 5 h / 20 °C / Inert atmosphere

With 1H-imidazole; peracetic acid; dmap; sodium tetrahydroborate; Wilkinson's catalyst; osmium(VIII) oxide; lithium borohydride; 2,6-di-tert-butyl-4-methylpyridine; mercury(II) diacetate; tetrabutyl ammonium fluoride; water; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; isopropyl alcohol; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; pyridine; ethanol; dichloromethane; water; acetone; acetonitrile; 5.1: Luche reduction / 12.1: Tamao oxidation;
DOI:10.1002/asia.200800429