2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

Base Information

Chemical Name:2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate
CAS No.:154345-11-6
Molecular Formula:C₁₄H₂₀BrF₃O₃SSi
Molecular Weight:433.362
Hs Code.:

Synonyms:2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

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Technology Process of 2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

There total 1 articles about 2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 154345-35-4
2-bromo-6-(tert-butyldimethylsilyl)-4-methylphenol

: 154345-11-6
2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 17.5h; Inert atmosphere;
DOI:10.1002/anie.200803011

Reference yield: 40.0%

: 1578-33-2
2-furyltrimethylsilane

: 154345-11-6
2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

: 1089666-07-8
5-tert-butyldimethylsilyl-1,4-epoxy-7-methyl-1-trimethylsilyl-1,4-dihydronaphthalene

Guidance literature:: With n-butyllithium; In hexane; toluene; at -78 ℃; for 0.25h; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200803011

Reference yield: 27.0%

: 17113-33-6
2-phenylfuran

: 154345-11-6
2-bromo-6-tert-butyldimethylsilyl-4-methylphenyl trifluoromethanesulfonate

: 1089666-05-6
5-tert-butyldimethylsilyl-1,4-epoxy-7-methyl-1-phenyl-1,4-dihydronaphthalene

: 1089666-06-7
8-tert-butyldimethylsilyl-1,4-epoxy-6-methyl-1-phenyl-1,4-dihydronaphthalene

Guidance literature:: With n-butyllithium; In hexane; toluene; at -78 ℃; for 0.333333h; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200803011