C₃₃H₅₄Si₂NIO₇

Base Information

Chemical Name:C₃₃H₅₄Si₂NIO₇
CAS No.:937164-16-4
Molecular Formula:C₃₃H₅₄INO₇Si₂
Molecular Weight:759.87
Hs Code.:

C<sub>33</sub>H<sub>54</sub>Si<sub>2</sub>NIO<sub>7</sub>

Synonyms:C₃₃H₅₄Si₂NIO₇

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Chemical Property of C₃₃H₅₄Si₂NIO₇

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Technology Process of C₃₃H₅₄Si₂NIO₇

There total 6 articles about C₃₃H₅₄Si₂NIO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 937163-78-5
C₁₇H₃₄SiO₄

: 937163-82-1
C₁₆H₂₁SiNO₃

: 937164-16-4
C₃₃H₅₄Si₂NIO₇

Guidance literature:: With N-iodo-succinimide; In dichloromethane; at 20 ℃;
DOI:10.1021/ol070435s

Reference yield:

: 937163-73-0
C₁₇H₃₄SiO₄

: 937164-16-4
C₃₃H₅₄Si₂NIO₇

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

2: 82 percent / NIS / CH₂Cl₂ / 20 °C

With N-iodo-succinimide; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol070435s

Reference yield:

: 937164-11-9
C₂₄H₃₈SiO₅

: 937164-16-4
C₃₃H₅₄Si₂NIO₇

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

2: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

3: 82 percent / NIS / CH₂Cl₂ / 20 °C

With N-iodo-succinimide; diisobutylaluminium hydride; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol070435s