Technology Process of C38H48N4O8
There total 5 articles about C38H48N4O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C39H50N4O8;
With
dihydrogen peroxide; lithium hydroxide;
In
methanol;
at 0 ℃;
With
hydrogenchloride; sodium thiosulfate;
In
methanol; water;
pH=1;
DOI:10.1016/j.tet.2011.11.089
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: methoxybenzene; trifluoroacetic acid / dichloromethane
2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C
3.2: pH 1
With
dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide;
In
methanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
2.1: methoxybenzene; trifluoroacetic acid / dichloromethane
3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 1 h / 20 °C / Inert atmosphere
4.1: dihydrogen peroxide; lithium hydroxide / methanol / 0 °C
4.2: pH 1
With
dihydrogen peroxide; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; lithium hydroxide;
In
methanol; dichloromethane;
DOI:10.1016/j.tet.2011.11.089