ethyl 3-(p-methoxyphenyl)nipecotate

Base Information

Chemical Name:ethyl 3-(p-methoxyphenyl)nipecotate
CAS No.:75910-85-9
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

Synonyms:ethyl 3-(p-methoxyphenyl)nipecotate

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Chemical Property of ethyl 3-(p-methoxyphenyl)nipecotate

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Technology Process of ethyl 3-(p-methoxyphenyl)nipecotate

There total 3 articles about ethyl 3-(p-methoxyphenyl)nipecotate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75910-83-7
ethyl 5-chloro-2-cyano-2-(p-methoxyphenyl)valerate

: 75910-85-9
ethyl 3-(p-methoxyphenyl)nipecotate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, NH₃(g), / Raney Ni, H₂PtCl₆*6H₂O / ethanol / 8 h / 2585.7 Torr

2: ethanol / 8 h / Heating

With ammonia; hydrogen; dihydrogen hexachloroplatinate; nickel; In ethanol;
DOI:10.1021/jm00134a020

Reference yield:

: 147795-54-8,15032-40-3
ethyl 2-cyano-2-(4-methoxyphenyl)acetate

: 75910-85-9
ethyl 3-(p-methoxyphenyl)nipecotate

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / potassium tert-butoxide / 2-methyl-propan-2-ol / 1.) RT, 24 h, 2.) reflux, 1 h

2: H₂, NH₃(g), / Raney Ni, H₂PtCl₆*6H₂O / ethanol / 8 h / 2585.7 Torr

3: ethanol / 8 h / Heating

With potassium tert-butylate; ammonia; hydrogen; dihydrogen hexachloroplatinate; nickel; In ethanol; tert-butyl alcohol;
DOI:10.1021/jm00134a020