cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

Base Information

Chemical Name:cis-4-(benzoyloxy)-2-cycloheptenyl benzoate
CAS No.:121921-26-4
Molecular Formula:C₂₁H₂₀O₄
Molecular Weight:336.387
Hs Code.:

Synonyms:cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

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Technology Process of cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

There total 3 articles about cis-4-(benzoyloxy)-2-cycloheptenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 876938-53-3
Cyclohepta-1,3-diene

: 65-85-0,8013-63-6
benzoic acid

: 121921-26-4
cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

: 121921-26-4,129584-27-6
trans-1,4-dibenzoyloxy-2-cycloheptene

Guidance literature:: With p-benzoquinone; palladium diacetate; In acetone; for 183h; Yield given. Yields of byproduct given; Ambient temperature;

Reference yield:

: 876938-53-3
Cyclohepta-1,3-diene

: 65-85-0,8013-63-6
benzoic acid

: 121921-26-4
cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

: 121921-26-4,129584-27-6
trans-1,4-dibenzoyloxy-2-cycloheptene

Guidance literature:: With p-benzoquinone; palladium diacetate; In acetone; for 183h; Yield given. Yields of byproduct given; Ambient temperature;

Reference yield:

: 876938-53-3
Cyclohepta-1,3-diene

: 65-85-0,8013-63-6
benzoic acid

: 957963-43-8
trans-cyclohept-2-ene-1,4-diyl dibenzoate

: 121921-26-4
cis-4-(benzoyloxy)-2-cycloheptenyl benzoate

Guidance literature:: Cyclohepta-1,3-diene; benzoic acid; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium hydroxide monohydrate; endo-tricyclo[6.2.2.0^2,7]dodeca-4,9-diene-3,6-dione; hydroquinone; In isopropyl alcohol; acetone; at 20 ℃; for 0.5h;

With tert.-butylhydroperoxide; In water; isopropyl alcohol; acetone; at 20 ℃; Overall yield = 65 %;
DOI:10.1021/acs.joc.5b02769