N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide
CAS No.:1370030-55-9
Molecular Formula:C₁₉H₁₆INO₃S
Molecular Weight:465.311
Hs Code.:

Synonyms:N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

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Chemical Property of N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

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Technology Process of N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

There total 4 articles about N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 869790-15-8
2-(2-iodophenoxy)aniline

: 98-59-9
p-toluenesulfonyl chloride

: 1370030-55-9
N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol3005134

Reference yield:

: 860465-22-1
1-iodo-2-(2-nitrophenoxy) benzene

: 1370030-55-9
N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride dihdyrate / ethyl acetate / 18 h / 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With pyridine; tin(II) chloride dihdyrate; In dichloromethane; ethyl acetate;
DOI:10.1021/ol3005134

Reference yield:

: 533-58-4
2-Iodophenol

: 1370030-55-9
N-[2-(2-iodophenoxy)phenyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / dimethyl sulfoxide / 100 °C / Inert atmosphere

2: tin(II) chloride dihdyrate / ethyl acetate / 18 h / 20 °C / Inert atmosphere

3: pyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With pyridine; tin(II) chloride dihdyrate; potassium carbonate; In dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/ol3005134