(Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

Base Information

Chemical Name:(Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester
CAS No.:87227-21-2
Molecular Formula:C₃₁H₃₇O₄P
Molecular Weight:504.606
Hs Code.:

(Triphenyl-λ<sup>5</sup>-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

Synonyms:(Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

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Chemical Property of (Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

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Technology Process of (Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

There total 2 articles about (Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 73818-55-0,15596-07-3
Bestmann ylide

: 87227-13-2
2-(8-Hydroxyoctyl)-1,3-dioxolan

: 87227-21-2
(Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

Guidance literature:: In toluene; for 48h; Heating;

Reference yield:

: 29541-97-7
9-acetoxynonal

: 87227-21-2
(Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) p-TsOH, 2.) 10percent KOH / 1.) toluene, reflux, 2.) MeOH, 30 deg C, 3 h

2: toluene / 24 h / Heating

With potassium hydroxide; toluene-4-sulfonic acid; In toluene;
DOI:10.1055/s-1989-27271

Reference yield:

: 87227-21-2
(Triphenyl-λ⁵-phosphanylidene)-acetic acid 8-[1,3]dioxolan-2-yl-octyl ester

: 1725-03-7
oxacyclododecan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 0.1 N HCl, THF / 1 h / Ambient temperature

2: LiOH, 85 percent H₃PO₄, glacial acetic acid, B(OH)3 / toluene; H₂O / pH 8.4

3: LiOH, 85 percent H₃PO₄, glacial acetic acid, B(OH)3 / toluene; H₂O / pH 8.4

4: 99 percent / H₂ / Pd/C

With tetrahydrofuran; hydrogenchloride; lithium hydroxide; phosphoric acid; hydrogen; boric acid; acetic acid; palladium on activated charcoal; In water; toluene;