ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

Base Information

Chemical Name:ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate
CAS No.:1374015-64-1
Molecular Formula:C₂₄H₂₇NO₃
Molecular Weight:377.483
Hs Code.:

Synonyms:ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

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Chemical Property of ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

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Technology Process of ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

There total 4 articles about ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53588-97-9
ethyl 2-(chlorocarbonyl)-3-phenylpropanoate

: 1279722-89-2
2-(cyclopentylidenemethyl)benzenamine

: 1374015-64-1
ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

Guidance literature:: With dmap; In toluene; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2012.03.004

Reference yield:

: 10299-81-7
1-(cyclopentylidenemethyl)-2-nitrobenzene

: 1374015-64-1
ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: iron; acetic acid / 70 °C

2: dmap / toluene / 0.08 h / 20 °C

With dmap; iron; acetic acid; In toluene;
DOI:10.1016/j.tet.2012.03.004

Reference yield:

: 2562-38-1
nitrocyclopentane

: 1374015-64-1
ethyl 2-benzyl-3-(2-(cyclopentylidenemethyl)phenylamino)-3-oxopropanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / dimethyl sulfoxide / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere; UV-irradiation

2.1: sodium hydride / dimethyl sulfoxide / 20 °C / Inert atmosphere

3.1: iron; acetic acid / 70 °C

4.1: dmap / toluene / 0.08 h / 20 °C

With dmap; iron; sodium hydride; acetic acid; In dimethyl sulfoxide; toluene;
DOI:10.1016/j.tet.2012.03.004