2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

Base Information

Chemical Name:2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde
CAS No.:1242157-12-5
Molecular Formula:C₁₉H₁₆BrFN₂O₂
Molecular Weight:403.251
Hs Code.:

Synonyms:2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

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Chemical Property of 2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

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Technology Process of 2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

There total 2 articles about 2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1242156-59-7
6-(tert-butyl)-8-fluorophthalazin-1(2H)-one

: 360575-28-6
2-bromo-6-fluorobenzaldehyde

: 1242157-12-5
2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

Guidance literature:: With Trimethylmethoxysilane; caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 4h;

Reference yield:

: 1242156-59-7
6-(tert-butyl)-8-fluorophthalazin-1(2H)-one

: 67713-23-9
2,6-dibromobenzaldehyde

: 1242157-12-5
2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

Guidance literature:: With copper(l) iodide; 4,7-dimethoxy-1,10-phenanthroline; caesium carbonate; In 1,4-dioxane; at 100 ℃; Inert atmosphere of nitrogen;

Reference yield: 89.0%

: 1242157-12-5
2-bromo-6-(6-tert-butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)benzaldehyde

: 1242156-70-2
2-methyl-2-{6-[1-methyl-2-oxo-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1,2-dihydro-pyridin-3-ylamino]-pyridin-3-yl}-propionic acid methyl ester

: 1242156-72-4
2-(6-{5-[3-(6-tert-Butyl-8-fluoro-1-oxo-1H-phthalazin-2-yl)-2-formyl-phenyl]-1-methyl-2-oxo-1,2-dihydro-pyridin-3-ylamino}-pyridin-3-yl)-2-methyl-propionic acid methyl ester

Guidance literature:: With caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; at 100 ℃; for 1h; Inert atmosphere of nitrogen;