Technology Process of C27H46O3S2Si
There total 6 articles about C27H46O3S2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
camphor-10-sulfonic acid;
In
methanol; dichloromethane;
at -10 ℃;
for 1h;
DOI:10.1002/anie.201201395
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium / tetrahydrofuran; pentane / 0.5 h / -78 - -40 °C / Inert atmosphere
2: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / -10 °C / Inert atmosphere
3: camphor-10-sulfonic acid / methanol; dichloromethane / 1 h / -10 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; camphor-10-sulfonic acid; tert.-butyl lithium; sodium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; pentane;
DOI:10.1002/anie.201201395
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 1 h / Cooling with ice
2: N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium / tetrahydrofuran; pentane / 0.5 h / -78 - -40 °C / Inert atmosphere
3: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / -10 °C / Inert atmosphere
4: camphor-10-sulfonic acid / methanol; dichloromethane / 1 h / -10 °C
With
N,N,N,N,N,N-hexamethylphosphoric triamide; camphor-10-sulfonic acid; tert.-butyl lithium; sodium hexamethyldisilazane; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; pentane;
DOI:10.1002/anie.201201395
