Technology Process of 5-(1-methyl-pentyl)-resorcinol
There total 7 articles about 5-(1-methyl-pentyl)-resorcinol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) sodium ethoxide / 1.) ethanol, 25 deg C, 2.5 h, 2.) ethanol, ambient temperature, 72 h
2: 93 percent / KOH / methanol / 6 h / 65 °C
3: 99 percent / H2 / Pd on carbon / ethanol / 20 h / 2327.2 Torr
4: 95 percent / LiAlH4 / tetrahydrofuran / 16 h / 0 - 20 °C
5: 62 percent / pyridine / CHCl3 / 3 h / 0 °C
6: 89 percent / Li2CuCl4 / tetrahydrofuran; diethyl ether / 16 h / -78 - 25 °C
7: 99 percent / boron tribromide / CH2Cl2 / 0 - 25 °C
With
pyridine; potassium hydroxide; lithium aluminium tetrahydride; dilithium tetrachlorocuprate; hydrogen; sodium ethanolate; boron tribromide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform;
DOI:10.1016/S0040-4020(96)01134-9
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / H2 / Pd on carbon / ethanol / 20 h / 2327.2 Torr
2: 95 percent / LiAlH4 / tetrahydrofuran / 16 h / 0 - 20 °C
3: 62 percent / pyridine / CHCl3 / 3 h / 0 °C
4: 89 percent / Li2CuCl4 / tetrahydrofuran; diethyl ether / 16 h / -78 - 25 °C
5: 99 percent / boron tribromide / CH2Cl2 / 0 - 25 °C
With
pyridine; lithium aluminium tetrahydride; dilithium tetrachlorocuprate; hydrogen; boron tribromide;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; chloroform;
DOI:10.1016/S0040-4020(96)01134-9
