PROPIONYL-3,3,3-D3 CHLORIDE

Base Information

• Chemical Name: PROPIONYL-3,3,3-D3 CHLORIDE
• CAS No.: 75695-44-2
• Molecular Formula: C₃H₅ClO
• Molecular Weight: 95.5013
• Mol file: 75695-44-2.mol

Synonyms:PROPIONYL-3,3,3-D3 CHLORIDE

Chemical Property of PROPIONYL-3,3,3-D3 CHLORIDE

Chemical Property:

• PSA: 17.07000
• LogP: 1.16180

Purity/Quality:

99% ^*data from raw suppliers

Propionyl-3,3,3-d3Chloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PROPIONYL-3,3,3-D3 CHLORIDE

There total 1 articles about PROPIONYL-3,3,3-D3 CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

<3,3,3-2H3>propionic acid (55577-88-3) → <3,3,3-2H3>propionyl chloride (75695-44-2)

Guidance literature:

With benzoyl chloride;

DOI:10.1039/P29950000119

Reference yield:

<3,3,3-2H3>propionyl chloride (75695-44-2) → <3,3,3-D3>-1-Propanol (61844-01-7)

Guidance literature:

With lithium aluminium tetrahydride; Tetraethylene glycol; In various solvent(s); at 30 - 50 ℃; overnight;

DOI:10.1002/oms.1210281035

Reference yield:

2.6-dimethylphenol (576-26-1,25134-01-4) + <3,3,3-2H3>propionyl chloride (75695-44-2) → 2',6'-dimethylphenyl-<3-2H3>-propionate (156451-04-6)

Guidance literature:

DOI:10.1016/S0040-4039(00)76544-0

upstream raw materials:

<3,3,3-2H3>propionic acid

Downstream raw materials:

2',6'-dimethylphenyl-<3-2H3>-propionate

<3,3,3-D3>-1-Propanol

Refernces

• 1、 Bowen, Richard D.,Suh, Dennis,Terlouw, Johan K.. "Mechanism of Propene and Water Elimination from the Oxonium Ion CH3CH=O+CH2CH2CH3". . p. 119 - 130. Retrieved 2007/10/02.
• 2、 Clezy, Peter S.,Ravi,B. N.,Thuc, Le van. "The Chemistry of Pyrrolic Compounds.LIX. The Oxidative Cyclization of Bilenes-b Substituted by Ethyl or Propyl Groups at a Terminal Site". . p. 419 - 432. Retrieved 2007/10/02.