bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)]

Base Information

Chemical Name:bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)]
CAS No.:74417-82-6
Molecular Formula:C₂₀H₃₀Cl₂O₂Pd₂
Molecular Weight:586.203
Hs Code.:

Synonyms:bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)]

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Technology Process of bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)]

There total 1 articles about bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 3792-53-8,4584-09-2,5524-05-0,5948-04-9,6909-25-7,7764-50-3,53796-79-5,69460-46-4,116499-64-0,619-02-3,619-01-2
2-methyl-5-(prop-1-en-2-yl)cyclohexanone

: palladium(II) trifluoroacetate

: 74417-82-6
bis[chloro(1',2',3'-trihapto-5-isopropenyl-2-methylcyclohexanone)palladium (II)]

Guidance literature:: With tetrabutyl-ammonium chloride; In acetone; byproducts: Pd, CF3COOH; under N2; stirred at ambient temperature for 15 h (overnight); Bu4NCl was added; stirred for 10 min; filtered; solvent was removed in vacuo; TLC (hexane-ethyl acetate); recrystallized from hexane-chloroform; elem. anal.;
DOI:10.1021/ja00530a042