[14C-formyl]-N-methylformanilide

Base Information

• Chemical Name: [14C-formyl]-N-methylformanilide
• CAS No.: 53197-55-0
• Molecular Formula: C₈H₉NO
• Molecular Weight: 137.155
• Mol file: 53197-55-0.mol

Synonyms:[14C-formyl]-N-methylformanilide

Chemical Property of [14C-formyl]-N-methylformanilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [14C-formyl]-N-methylformanilide

There total 2 articles about [14C-formyl]-N-methylformanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

N-methylaniline (100-61-8) + benzyl [14C]-formate → [14C-formyl]-N-methylformanilide (53197-55-0)

Guidance literature:

at 95 ℃; for 48h;

DOI:10.1021/ja0111479

Reference yield:

N-methylaniline (100-61-8) + sodium [14C]formate (2792-70-3) → [14C-formyl]-N-methylformanilide (53197-55-0)

Guidance literature:

sodium [14C]formate; With formic acid; In dichloromethane; at 20 ℃; for 0.333333h; sonication;

N-methylaniline; With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1002/jlcr.806

Reference yield: 44.0%

1-bromo-4-methoxy-benzene (104-92-7) + [14C-formyl]-N-methylformanilide (53197-55-0) → 4-methoxy-benzaldehyde-[carbonyl-14C] (35947-48-9)

Guidance literature:

1-bromo-4-methoxy-benzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 0.166667h;

[14C-formyl]-N-methylformanilide; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1002/jlcr.806

upstream raw materials:

N-methylaniline

sodium [14C]formate

Downstream raw materials:

4-methoxy-benzaldehyde-[carbonyl-14C]