Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine

Base Information

• Chemical Name: Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine
• CAS No.: 1059138-20-3
• Molecular Formula: C₃₀H₃₈N₄O₈
• Molecular Weight: 582.654

Synonyms:Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine

Chemical Property of Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine

Chemical Property:

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Technology Process of Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine

There total 1 articles about Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine methyl ester (1059138-18-9) → Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine (1059138-20-3)

Guidance literature:

With sodium hydroxide; water; In tetrahydrofuran; methanol; at 0 - 20 ℃;

DOI:10.1021/ja805647k

Reference yield: 77.0%

Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine (1059138-20-3) → Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-(Z)-α,β-dehydro-L-phenylalanine azlactone (1059138-22-5)

Guidance literature:

With sodium acetate; acetic anhydride; In tetrahydrofuran; at 20 ℃; for 48h;

DOI:10.1021/ja805647k

upstream raw materials:

Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-3-phenyl-L-serine methyl ester

Downstream raw materials:

Boc-β-Ala-((Z)-α,β-dehydro-L-phenylalanyl)-(α-aminoisobutyryl)-(Z)-α,β-dehydro-L-phenylalanine azlactone

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