benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

Base Information

Chemical Name:benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside
CAS No.:352211-76-8
Molecular Formula:C₃₅H₃₆O₅
Molecular Weight:536.668
Hs Code.:

Synonyms:benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

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Chemical Property of benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

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Technology Process of benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

There total 3 articles about benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 352211-75-7
benzyl 2,4,6-tri-O-benzyl-β-D-xylo-hex-3-ulopyranoside

: 352211-76-8
benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

Guidance literature:: In tetrahydrofuran; toluene; at 0 - 20 ℃;
DOI:10.1021/jo015543l

Reference yield:

: 62447-55-6
Benzyl 2,4,6-tri-O-benzyl-β-D-galactopyranoside

: 352211-76-8
benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h

2: 82 percent / toluene; tetrahydrofuran / 0 - 20 °C

With Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo015543l

Reference yield:

: 352211-74-6
benzyl 3-O-allyl-2,4,6-tri-O-benzyl-β-D-galactopyranoside

: 352211-76-8
benzyl 2,4,6-tri-O-benzyl-3-deoxy-3-C-methylene-β-D-xylo-hex-3-ulopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / Pd(PPh₃)4; sodium p-toluenesulfinate; HOAc / CH₂Cl₂ / 48 h / 20 °C

2: 98 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h

3: 82 percent / toluene; tetrahydrofuran / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; Dess-Martin periodane; acetic acid; sodium 4-methylbenzenesulfinate; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo015543l