C₆₂H₁₁₃O₁₃PSi₃

Base Information

Chemical Name:C₆₂H₁₁₃O₁₃PSi₃
CAS No.:1422462-98-3
Molecular Formula:C₆₂H₁₁₃O₁₃PSi₃
Molecular Weight:1181.8
Hs Code.:

C<sub>62</sub>H<sub>113</sub>O<sub>13</sub>PSi<sub>3</sub>

Synonyms:C₆₂H₁₁₃O₁₃PSi₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₂H₁₁₃O₁₃PSi₃

Chemical Property:

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Technology Process of C₆₂H₁₁₃O₁₃PSi₃

There total 32 articles about C₆₂H₁₁₃O₁₃PSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1422462-97-2
C₆₄H₁₁₅O₁₄PSi₃

: 1422462-98-3
C₆₂H₁₁₃O₁₃PSi₃

Guidance literature:: With methanol; barium hydroxide octahydrate; at 20 ℃; for 0.166667h;
DOI:10.1021/jo3026077

Reference yield:

: 1422462-85-8
C₂₆H₄₈O₅Si₂

: 1422462-98-3
C₆₂H₁₁₃O₁₃PSi₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.1: water; acetic acid / tetrahydrofuran / 0.67 h / 0 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

4.2: 16 h / 20 °C / Inert atmosphere

5.1: methanol; barium hydroxide octahydrate / 0.17 h / 20 °C

With methanol; barium hydroxide octahydrate; 2,4,6-trichlorobenzoyl chloride; water; acetic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo3026077

Reference yield:

: C₂₉H₄₈O₅Si

: 1422462-98-3
C₆₂H₁₁₃O₁₃PSi₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; sodium periodate / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

4.1: water; acetic acid / tetrahydrofuran / 0.67 h / 0 °C

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

5.2: 16 h / 20 °C / Inert atmosphere

6.1: methanol; barium hydroxide octahydrate / 0.17 h / 20 °C

With methanol; sodium periodate; barium hydroxide octahydrate; 2,4,6-trichlorobenzoyl chloride; water; acetic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo3026077