(η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II)

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Chemical Name:(η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II)
CAS No.:97689-56-0
Molecular Formula:C₂₈H₂₆MoO₃
Molecular Weight:506.453
Hs Code.:

Synonyms:(η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II)

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Technology Process of (η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II)

There total 1 articles about (η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: di[(pentamethylcyclopentadienyl)molybdenum]hexacarbonyl

: 37647-36-2
1,2-dophenylcyclopropenylim perchlorate

: 97689-56-0
(η-pentamethylcyclopentadienyl)(η3-2,3-diphenyloxocyclobutenyl)dicarbonylmolybdenum(II)

Guidance literature:: With sodium amalgam; In tetrahydrofuran; Mo dimer adding in soln. to Na amalgam under N2, stirring for 45 min, Hg draining off, filtering, filter washing with THF, combined washings cooling to -80°C, ClO4 salt adding, stirring for 1 h, warming to room temp., stirring overnight, evapg.; isolated by chromy. on Florisil column, purified by recrystallization from CH2Cl2-hexane, identified by elem. anal., IR and NMR spectra;