Technology Process of C39H58N2O11
There total 1 articles about C39H58N2O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: pyridinium p-toluenesulfonate / CH2Cl2
2.1: 60 percent / potassium bis(trimethylsilyl)amide / tetrahydrofuran / 0 °C
3.1: sodium borohydride; methanol / NiCl2*xH2O / 10 h / 0 °C
4.1: potassium carbonate / methanol / 72 h
5.1: triethylamine / CH2Cl2
5.2: aq. HCl / ethanol / 0.5 h / Heating
6.1: 63 percent / EDCI; pyridinium trifluoroacetate; DMSO / CH2Cl2
With
methanol; sodium tetrahydroborate; pyridinium trifluroacetate; pyridinium p-toluenesulfonate; potassium hexamethylsilazane; potassium carbonate; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
nickel dichloride;
In
tetrahydrofuran; methanol; dichloromethane;
4.1: Michael addition / 6.1: Pfitzner-Moffat reaction;
DOI:10.1016/j.tetlet.2005.01.126