Technology Process of C14H18O7
There total 4 articles about C14H18O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C13H18O5;
With
iron(III) chloride hexahydrate;
In
acetic acid;
for 2h;
Inert atmosphere;
acetic anhydride;
In
acetic acid;
for 3h;
Inert atmosphere;
DOI:10.1016/j.tet.2013.04.102
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere
2.1: iron(III) chloride hexahydrate / acetic acid / 2 h / Inert atmosphere
2.2: 3 h / Inert atmosphere
With
iron(III) chloride hexahydrate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
1,4-dioxane; acetic acid;
DOI:10.1016/j.tet.2013.04.102
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / toluene / 8 h / 20 °C / Inert atmosphere
2.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / -20 °C / Inert atmosphere
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 1 h / 20 °C / Inert atmosphere
4.1: iron(III) chloride hexahydrate / acetic acid / 2 h / Inert atmosphere
4.2: 3 h / Inert atmosphere
With
iron(III) chloride hexahydrate; potassium tert-butylate; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; 1,4-dioxane; acetic acid; toluene;
DOI:10.1016/j.tet.2013.04.102
