Technology Process of C20H32O2Si
There total 5 articles about C20H32O2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C17H26OSi;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 ℃;
for 0.166667h;
trimethylene oxide;
With
boron trifluoride diethyl etherate;
In
tetrahydrofuran;
at -78 ℃;
With
ammonium chloride;
In
water;
Saturated solution;
DOI:10.1021/ol201149u
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triphenylphosphine / dichloromethane / 1 h / 20 °C
1.2: 0.25 h / -78 °C
2.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C
2.2: -78 °C
2.3: Saturated solution
With
n-butyllithium; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
1.1: Corey-Fuchs reaction / 1.2: Corey-Fuchs reaction;
DOI:10.1021/ol201149u
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C
2.1: toluene-4-sulfonic acid / benzene / 1 h / 90 °C
3.1: ozone / methanol / 0.08 h / -78 °C
3.2: 12 h / 20 °C
4.1: triphenylphosphine / dichloromethane / 1 h / 20 °C
4.2: 0.25 h / -78 °C
5.1: n-butyllithium / tetrahydrofuran / 0.17 h / -78 °C
5.2: -78 °C
5.3: Saturated solution
With
sodium tetrahydroborate; n-butyllithium; toluene-4-sulfonic acid; ozone; triphenylphosphine;
In
tetrahydrofuran; methanol; dichloromethane; benzene;
4.1: Corey-Fuchs reaction / 4.2: Corey-Fuchs reaction;
DOI:10.1021/ol201149u