(S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

Base Information

Chemical Name:(S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate
CAS No.:1373883-27-2
Molecular Formula:C₂₁H₂₅N₃O₆
Molecular Weight:415.446
Hs Code.:

Synonyms:(S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

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Technology Process of (S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

There total 1 articles about (S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 33305-77-0
Boc-Phe(p-NO₂)-OH

: 90-04-0
2-methoxy-phenylamine

: 1373883-27-2
(S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

Guidance literature:: With bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 20h;
DOI:10.1002/anie.201106832

Reference yield: 98.0%

: 1373883-27-2
(S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

: 1373883-28-3
(S)-2-amino-N-(2-methoxyphenyl)-3-(4-nitrophenyl)propanamide hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane; cyclopentyl methyl ether; at 0 - 20 ℃; for 24h;
DOI:10.1002/anie.201106832

Reference yield:

: 1373883-27-2
(S)-tert-butyl (1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)carbamate

: 1373883-29-4
(S)-2-methoxy-N-(1-((2-methoxyphenyl)amino)-3-(4-nitrophenyl)-1-oxopropan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; cyclopentyl methyl ether / 24 h / 0 - 20 °C

2: triethylamine / dichloromethane / 0.25 h / 0 - 20 °C

With hydrogenchloride; triethylamine; In dichloromethane; cyclopentyl methyl ether;
DOI:10.1002/anie.201106832