4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

Base Information

Chemical Name:4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide
CAS No.:566920-33-0
Molecular Formula:C₂₀H₁₉NO₄
Molecular Weight:337.375
Hs Code.:

Synonyms:4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

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Chemical Property of 4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

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Technology Process of 4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

There total 4 articles about 4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-methyl-2-oxo-4-phenylpentanoic acid chloride

: 65399-05-5
5-amino-3H-isobenzofuran-1-one

: 566920-33-0
4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

Guidance literature:: In N,N-dimethyl acetamide; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2005.07.025

Reference yield:

: 2-phenyl-2,2-dimethylethylmagnesium bromide

: 566920-33-0
4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / N,N-dimethyl-acetamide / 0 °C

2: N,N-dimethyl-acetamide / 0 - 20 °C

With thionyl chloride; In N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2005.07.025

Reference yield:

: 217195-70-5
4-methyl-2-oxo-4-phenylpentanoic acid

: 566920-33-0
4-methyl-2-oxo-4-phenylpentanoic acid (1-oxo-1,3-dihydroisobenzofuran-5-yl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / N,N-dimethyl-acetamide / 0 °C

2: N,N-dimethyl-acetamide / 0 - 20 °C

With thionyl chloride; In N,N-dimethyl acetamide;
DOI:10.1016/j.bmcl.2005.07.025