C₅₇H₇₃N₃Si₂

Base Information

Chemical Name:C₅₇H₇₃N₃Si₂
CAS No.:1362020-00-5
Molecular Formula:C₅₇H₇₃N₃Si₂
Molecular Weight:856.398
Hs Code.:

C<sub>57</sub>H<sub>73</sub>N<sub>3</sub>Si<sub>2</sub>

Synonyms:C₅₇H₇₃N₃Si₂

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Chemical Property of C₅₇H₇₃N₃Si₂

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Technology Process of C₅₇H₇₃N₃Si₂

There total 16 articles about C₅₇H₇₃N₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1362020-07-2
C₆₆H₉₃N₃Si₃

: 1362020-00-5
C₅₇H₇₃N₃Si₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201102031

Reference yield:

: 475160-70-4
4-(diisopropylsilanyl)-phenyl methanol

: 1362020-00-5
C₅₇H₇₃N₃Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: manganese(IV) oxide / dichloromethane / 5 h / 20 °C / Inert atmosphere

2.1: potassium tert-butylate / toluene / 12 h / Inert atmosphere; Reflux

3.1: Wilkinson's catalyst; sodium iodide / toluene / 16 h / Inert atmosphere; Reflux

4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

4.2: 3 h / -78 - 20 °C / Inert atmosphere

5.1: Wilkinson's catalyst; sodium iodide / toluene / 16 h / Inert atmosphere; Reflux

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With manganese(IV) oxide; Wilkinson's catalyst; n-butyllithium; potassium tert-butylate; tetrabutyl ammonium fluoride; sodium iodide; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1002/chem.201102031

Reference yield:

: 1362019-95-1
4-bromo-4'-(diisopropylsilyl)-E-stilbene

: 1362020-00-5
C₅₇H₇₃N₃Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: Wilkinson's catalyst; sodium iodide / toluene / 16 h / Inert atmosphere; Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 - 20 °C / Inert atmosphere

3.1: Wilkinson's catalyst; sodium iodide / toluene / 16 h / Inert atmosphere; Reflux

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With Wilkinson's catalyst; n-butyllithium; tetrabutyl ammonium fluoride; sodium iodide; In tetrahydrofuran; hexane; toluene;
DOI:10.1002/chem.201102031