methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

Base Information

Chemical Name:methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside
CAS No.:109049-71-0
Molecular Formula:C₂₆H₂₈O₅
Molecular Weight:421.497
Hs Code.:

Synonyms:methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

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Chemical Property of methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

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Technology Process of methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

There total 3 articles about methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 109049-70-9
methyl 2,3-anhydro-5-O-(4-methoxytriphenylmethyl)-β-D-lyxofuranoside

: 109049-71-0
methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

: 109049-72-1
C₂₆H₂₇⁽²⁾HO₅

Guidance literature:: With lithium aluminium deuteride; In tetrahydrofuran; at 0 ℃; for 6h;
DOI:10.1016/S0040-4020(01)82094-9

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 109049-71-0
methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / 20 °C

2: 82 percent / lithium aluminium hydride / tetrahydrofuran / 6 h / 0 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine;
DOI:10.1016/S0040-4020(01)82094-9

Reference yield:

: 43168-73-6
methyl 2,3-anhydro-β-D-lyxofuranoside

: 109049-71-0
methyl 2-deoxy-2(R)-deuterio-5-O-(4-methoxytriphenylmethyl)-β-D-threo-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / pyridine / 20 °C

2: 82 percent / lithium aluminium hydride / tetrahydrofuran / 6 h / 0 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine;
DOI:10.1016/S0040-4020(01)82094-9